Published September Origi- nally approved in Last previous edition approved in as 3. E – 89a (). Annual Book of ASTM Standards. Buy ASTM E TEST METHODS FOR CHEMICAL ANALYSIS OF COPPER ALLOYS from SAI Global. These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for.

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Add 50 mL of hot water and, if the solution is clear, proceed as described in If the entire electrolyte is to be used, proceed directly with the neutralization. Using a pH meter, check the pH of the solution which should be between 5.

ASTM E – 08() Standard Test Methods for Chemical Analysis of Copper Alloys

zstm Using indicator paper, check the pH, which should be between 6. Add mL of water and 2 to 3 g of iron powder. Add 5 mL more of diethyldithiocarbamate solution to the separatory funnel and mix. It is the responsibility of asm user of this zstm to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Current edition approved August 10, Search book title Enter keywords for book title search. Cautiously add formaldehyde solution, 1 to 2 mL at a time, until the color has changed again to wine red. If enough tin is present at this point to cause turbidity, proceed as directed to When dissolution is complete, heat the solution to boiling and continue to boil until oxides of nitrogen are removed.


Shake the separatory funnel vigorously for 30 s and allow the phases to separate. Do not use a solution that has stood more than 1 week. Proceed as directed in Astmm bronze NIST 52c, 0. Standards Subsctiption may be the perfect solution. ASTM D astmimportantespara la destilacion a presiones inferiores de 1 atm, archivo actualizadoen la ultima version.

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E 32 – latest. Las Lastt pre previo vious us edi editio tionn ap appro prove vedd in 19 96 as E — 89a Cover the beaker with a plastic cover and allow the sample to dissolve.

If the minimum requirements are not met with the selected calibration solutions, do not use this method until the desired stability is obtained. Prepare fresh e487 needed.

Standard Test Methods for Chemical Analysis of Copper Alloys

Your Alert Profile lists the documents that will be monitored. Precipitate the iron and tin as before and heat to boiling to coagulate the precipitate. Calculate the percentage of nickel as follows: E Standard Terminology Relating to Metallography. The surface of the platinum electrodes should be smooth, clean and bright to promote uniform deposition and good adherence.

Cool, dilute to volume, and mix. One of the simplest methods is by means of the apparatus shown in Fig. Calculate the percentage of tin as follows: Work in a well-ventilated hood. Cover the beaker with a ribbed cover glass. Your consent to our cookies if you continue to use this website. Cool until the violent reaction has ceased.


It is expected that work will be performed in a properly equipped laboratory.

Using a pH meter, check the pH; if it is not between 6. Titrate dropwise until the color changes from purplish-red to yellow. Discard the organic layer. Asrm in a polyethylene bottle. This standard is not included in any packages. Add 10 mL of HCl and dilute to 1 L.

Stir the wstm vigorously and allow xstm cool to room temperature while stirring occasionally. The zinc is then stripped from the organic phase as the ammonia complex, which is further treated with potassium cyanide to complex bivalent metals as well as the zinc.

Allow the layers to separate; draw off the lower organic layer into a mL beaker, retaining the aqueous layer. Users are encouraged to employ suitable reference materials, if available, to verify the accuracy of the method in their laboratories.

Dilute to 20 mL. Heat to copious white fumes and boil to destroy organic matter.